Answer:
(a) (i) Methyl 3-chlorobut-2-en-1-oate (ii) 3-Methylcyclohexyne
(b) has significant dipole moment while being symmetrical has zero dipole moment. Therefore, di-tert-butyl benzene is non-polar and hence will not be adsorbed strongly on the adsorbent and hence it will be eluted first in moderately polar solvent.
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